2-benzyl-5-hexenoic acid allylbenzyloxyamide

Base Information

Chemical Name:2-benzyl-5-hexenoic acid allylbenzyloxyamide
CAS No.:1259429-84-9
Molecular Formula:C₂₃H₂₇NO₂
Molecular Weight:349.473
Hs Code.:

Synonyms:2-benzyl-5-hexenoic acid allylbenzyloxyamide

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Chemical Property of 2-benzyl-5-hexenoic acid allylbenzyloxyamide

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Technology Process of 2-benzyl-5-hexenoic acid allylbenzyloxyamide

There total 1 articles about 2-benzyl-5-hexenoic acid allylbenzyloxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1105107-68-3
2-benzylhex-5-enoic acid

: 122149-19-3
N-allyl-O-benzylhydroxylamine

: 1259429-84-9
2-benzyl-5-hexenoic acid allylbenzyloxyamide

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo101805q

Reference yield: 31.0%

: 1259429-84-9
2-benzyl-5-hexenoic acid allylbenzyloxyamide

: 1259429-86-1
3-benzyl-1-benzyloxy-2,4,5,8-tetrahydro-1H-azocine-2-one

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; for 16h; Reflux;
DOI:10.1021/jo101805q

Reference yield:

: 1259429-84-9
2-benzyl-5-hexenoic acid allylbenzyloxyamide

: 1227635-46-2
α-benzyl-N-methoxycarbonylazepane

Guidance literature:: Multi-step reaction with 4 steps

1: Grubbs catalyst first generation / dichloromethane / 16 h / Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 2 h

3: dmap; triethylamine / N,N-dimethyl-formamide / 3 h

4: triethylamine / 6 h / -78 - 20 °C / UV-irradiation

With Grubbs catalyst first generation; dmap; palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo101805q