1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

Base Information

Chemical Name:1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside
CAS No.:123573-98-8
Molecular Formula:C₅₃H₈₃NO₁₁
Molecular Weight:910.242
Hs Code.:

Synonyms:1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

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Chemical Property of 1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

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Technology Process of 1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

There total 8 articles about 1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-((4aR,6S,7R,8R,8aS)-2,2-Dimethyl-7-tetradecanoylamino-8-tetradecanoyloxy-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-pentanedioic acid dibenzyl ester

: 123573-98-8
1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: With acetic acid; at 90 ℃; for 0.333333h; Yield given;
DOI:10.1248/cpb.39.3244

Reference yield:

: 100-39-0
benzyl bromide

: 123573-98-8
1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / dimethylformamide / 24 h / Ambient temperature

2: 80 percent / p-TsOH*H₂O / acetone

3: DMAP, DCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 90percent aq. AcOH / 0.33 h / 90 °C

With dmap; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.39.3244

Reference yield:

: 133339-62-5
1,3-Di(methyloxycarbonyl)isopropyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 123573-98-8
1,3-di(benzyloxycarbonyl)isopropyl 2-deoxy-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: Zn, AcOH / 1 h / Ambient temperature

2: DCC / CH₂Cl₂ / 1 h / Ambient temperature

3: LiOH*H₂O / methanol; H₂O / 12 h / Ambient temperature

4: NaHCO₃ / dimethylformamide / 24 h / Ambient temperature

5: 80 percent / p-TsOH*H₂O / acetone

6: DMAP, DCC / CH₂Cl₂ / 2 h / Ambient temperature

7: 90percent aq. AcOH / 0.33 h / 90 °C

With dmap; lithium hydroxide; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.39.3244