2,4,6-trithiophenobarbital

Base Information

• Chemical Name: 2,4,6-trithiophenobarbital
• CAS No.: 30006-29-2
• Molecular Formula: C₁₂H₁₂N₂S₃
• Molecular Weight: 280.439

Synonyms:2,4,6-trithiophenobarbital

Chemical Property of 2,4,6-trithiophenobarbital

Chemical Property:

Purity/Quality:

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Technology Process of 2,4,6-trithiophenobarbital

There total 5 articles about 2,4,6-trithiophenobarbital which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

phenobarbital (50-06-6) → 2,4,6-trithiophenobarbital (30006-29-2)

Guidance literature:

With tetraphosphorus decasulfide; In methoxybenzene; for 8h; Heating;

Reference yield: 55.0%

phenobarbital (50-06-6) → 2,4,6-trithiophenobarbital (30006-29-2) + 5-ethyl-5-phenyl-2-thiobarbituric acid (2753-74-4) + 2,4-dithiophenobarbital (30006-28-1) + 4-thiophenobarbital (60024-01-3)

Guidance literature:

With Lawessons reagent; In methoxybenzene; for 4h; Heating;

Reference yield:

phenobarbital (50-06-6) → 2,4,6-trithiophenobarbital (30006-29-2) + 2,4-dithiophenobarbital (30006-28-1)

Guidance literature:

With tetraphosphorus decasulfide; xylene;

DOI:10.1039/jr9440000124

upstream raw materials:

phenobarbital

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