C₂₇H₃₇N₅O₆

Base Information

Chemical Name:C₂₇H₃₇N₅O₆
CAS No.:1438021-06-7
Molecular Formula:C₂₇H₃₇N₅O₆
Molecular Weight:527.621
Hs Code.:

C<sub>27</sub>H<sub>37</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₂₇H₃₇N₅O₆

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Chemical Property of C₂₇H₃₇N₅O₆

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Technology Process of C₂₇H₃₇N₅O₆

There total 7 articles about C₂₇H₃₇N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1438020-91-7
C₂₁H₂₆N₂O₅

: 219511-71-4
tert-butyl carbamimidoylcarbamate

: 1438021-06-7
C₂₇H₃₇N₅O₆

Guidance literature:: C₂₁H₂₆N₂O₅; With 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

tert-butyl carbamimidoylcarbamate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/ja4025148

Reference yield:

: 1438020-58-6
C₂₀H₂₃NO₆

: 1438021-06-7
C₂₇H₃₇N₅O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C

2.2: 12 h / 20 °C

3.1: trifluoroacetic acid; hydrogenchloride / dichloromethane; water / 12 h / 20 °C

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / 20 °C

4.2: 12 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; formic acid; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148

Reference yield:

: 1438020-52-0
C₁₆H₁₇NO₄

: 1438021-06-7
C₂₇H₃₇N₅O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; bromine; sulfuryl dichloride / 5 h / 10 - 20 °C

1.2: 1 h / 20 °C

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h

3.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C

4.2: 12 h / 20 °C

5.1: trifluoroacetic acid; hydrogenchloride / dichloromethane; water / 12 h / 20 °C

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / 20 °C

6.2: 12 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; formic acid; sulfuryl dichloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; bromine; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148