Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

Base Information

Chemical Name:Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2
CAS No.:133851-92-0
Molecular Formula:C₂₇H₃₂N₄O₆
Molecular Weight:508.574
Hs Code.:

Synonyms:Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

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Chemical Property of Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

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Technology Process of Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

There total 2 articles about Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98900-24-4
tert-butyl 2-[2-(1,3-dioxoisoindolin-2-yl)ethoxy]acetate

: 133851-92-0
Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / trifluoroacetic acid (TFA) / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 1.) N-methylmorpholine (NMM), isobutyl chloroformate (IBCF), 2.) NMM / 1.) DMF, -25 deg C, 5 min, 2.) DMF, -20 deg C

With 4-methyl-morpholine; trifluoroacetic acid; isobutyl chloroformate; In dichloromethane;
DOI:10.1021/jm00112a018

Reference yield:

: 69676-65-9
2-(2-phthalimidoethoxy)-acetic acid

: 81638-86-0
(S)-2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanamide hydrochloride

: 133851-92-0
Pht-GlyΨ(CH2O)Gly-Phe-Leu-NH2

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; Yield given. Multistep reaction; 1.) DMF, -25 deg C, 5 min, 2.) DMF, -20 deg C;
DOI:10.1021/jm00112a018