benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

Base Information

Chemical Name:benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate
CAS No.:1246303-78-5
Molecular Formula:C₂₀H₁₅N₃O₆
Molecular Weight:393.356
Hs Code.:

Synonyms:benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

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Chemical Property of benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

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Technology Process of benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

There total 1 articles about benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1246303-70-7
benzyl 2,4-dioxopiperidine-1-carboxylate

: 1011-84-3
4-nitrobenzohydroximoyl chloride

: 1246303-78-5
benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

Guidance literature:: benzyl 2,4-dioxopiperidine-1-carboxylate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

4-nitrobenzohydroximoyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 5h;
DOI:10.1002/chem.201001492

Reference yield: 73.0%

: 1246303-78-5
benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

: 1246303-88-7
benzyl 3-(4-aminophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

Guidance literature:: With acetic acid; zinc; In dichloromethane; at 0 ℃;
DOI:10.1002/chem.201001492

Reference yield:

: 1246303-78-5
benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate

: 1246303-85-4
C₂₀H₁₇N₃O₇

Guidance literature:: benzyl 3-(4-nitrophenyl)-4-oxo-6,7-dihydroisoxazolo[4,5-c]pyridine-5(4H)-carboxylate; With water; sodium hydroxide; In tetrahydrofuran; at 40 ℃;

With citric acid; In tetrahydrofuran; water;
DOI:10.1002/chem.201001492