2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

Base Information

Chemical Name:2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside
CAS No.:118638-77-0
Molecular Formula:C₃₅H₅₅NO₁₀
Molecular Weight:649.822
Hs Code.:

Synonyms:2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

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Chemical Property of 2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

Chemical Property:

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Technology Process of 2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

There total 4 articles about 2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 118638-77-0
2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH*H₂O / CHCl₃ / 6.5 h / Heating

2: 1) K₂CO₃, Et₃O*BF₄, 2) 1 M HCl / 1) CH₂Cl₂, room temperature, 17.5 h, 2) THF, room temperature, 40 min

3: Et₃N

With hydrogenchloride; triethyloxonium fluoroborate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In chloroform;
DOI:10.1248/cpb.38.3366

Reference yield:

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3
2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose

: 118638-77-0
2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: CaSO₄, BF₃*Et₂O / CH₂Cl₂ / 19 h / Ambient temperature

2: p-TsOH*H₂O / CHCl₃ / 6.5 h / Heating

3: 1) K₂CO₃, Et₃O*BF₄, 2) 1 M HCl / 1) CH₂Cl₂, room temperature, 17.5 h, 2) THF, room temperature, 40 min

4: Et₃N

With hydrogenchloride; calcium sulfate; boron trifluoride diethyl etherate; triethyloxonium fluoroborate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In dichloromethane; chloroform;
DOI:10.1248/cpb.38.3366

Reference yield:

: 118638-76-9
2-O-benzyloxyethyl-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 118638-77-0
2-benzyloxyethyl 3,4,6-tri-O-acetyl-2-deoxy-2-tetradecanoylamino-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) K₂CO₃, Et₃O*BF₄, 2) 1 M HCl / 1) CH₂Cl₂, room temperature, 17.5 h, 2) THF, room temperature, 40 min

2: Et₃N

With hydrogenchloride; triethyloxonium fluoroborate; potassium carbonate; triethylamine;
DOI:10.1248/cpb.38.3366