(E)-1-(2-bromovinyl)-3-methoxybenzene

Base Information

Chemical Name:(E)-1-(2-bromovinyl)-3-methoxybenzene
CAS No.:77150-94-8
Molecular Formula:C₉H₉BrO
Molecular Weight:213.074
Hs Code.:

Synonyms:(E)-1-(2-bromovinyl)-3-methoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(2-bromovinyl)-3-methoxybenzene

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Technology Process of (E)-1-(2-bromovinyl)-3-methoxybenzene

There total 12 articles about (E)-1-(2-bromovinyl)-3-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 6099-04-3,17570-26-2
3-methoxycinnamic acid

: 77150-94-8
(E)-1-(2-bromovinyl)-3-methoxybenzene

Guidance literature:: 3-methoxycinnamic acid; With lithium acetate; In water; acetonitrile; at 20 ℃; for 0.0833333h;

With N-Bromosuccinimide; In water; acetonitrile; at 20 ℃;
DOI:10.1021/acs.joc.8b00150

Reference yield:

: 874-98-6
1-bromomethyl-3-methoxybenzene

: 74-95-3
1,1-dibromomethane

: 77150-94-8
(E)-1-(2-bromovinyl)-3-methoxybenzene

Guidance literature:: 1,1-dibromomethane; With sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.333333h; Schlenk technique; Inert atmosphere;

1-bromomethyl-3-methoxybenzene; In tetrahydrofuran; diethyl ether; at -78 - 25 ℃; for 3h; Schlenk technique; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; diethyl ether; at 25 ℃; for 1h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b04004

Reference yield:

: 253684-23-0
1,1-dibromo-2-(3-methoxyphenyl)ethene

: 77150-94-8
(E)-1-(2-bromovinyl)-3-methoxybenzene

: 115665-63-9
(Z)-1-(2-bromovinyl)-3-methoxybenzene

Guidance literature:: With sodium ethanolate; phosphonic acid diethyl ester; In ethanol; for 0.0166667h; Title compound not separated from byproducts; microwave irradiation;
DOI:10.1016/S0040-4020(02)00013-3