methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

Base Information

Chemical Name:methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate
CAS No.:561007-53-2
Molecular Formula:C₁₇H₂₆NO₆P
Molecular Weight:371.37
Hs Code.:

Synonyms:methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

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Chemical Property of methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

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Technology Process of methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

There total 1 articles about methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 109638-99-5
(+/-)-1-benzyloxycarbonylamino-3-methylbutylphosphonous acid

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 561007-53-2
methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

Guidance literature:: (+/-)-1-benzyloxycarbonylamino-3-methylbutylphosphonous acid; With 1,1,1,3,3,3-hexamethyl-disilazane; at 100 - 110 ℃; for 2h;

acrylic acid methyl ester; at 85 - 90 ℃; for 3h;
DOI:10.1021/jm030795v

Reference yield: 90.0%

: 768-90-1
1-Adamantyl bromide

: 561007-53-2
methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

: methyl 3-[(1-N-(benzyloxycarbonylamino)-3-methylbutyl)adamantyloxyphoshinyl]propanoate

Guidance literature:: With silver(l) oxide; In chloroform; at 65 ℃; for 4h;
DOI:10.3390/ijms22105090

Reference yield:

: 561007-53-2
methyl 3-{[1-(N-benzyloxycarbonylamino)-3-methylbutyl]hydroxyphosphinyl}propionate

: (R)-(-)-Z-Leuψ(PO2HCH2)GlyOMe

: (S)-(+)-Z-Leuψ(PO2HCH2)GlyOMe

Guidance literature:: With sodium dihydrogen phosphate; Chiral AX QD-1 stationary phase; In methanol; water; at 20 ℃; pH=5.6;
DOI:10.1016/S0957-4166(03)00537-8