N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Base Information

Chemical Name:N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt
CAS No.:96948-40-2
Molecular Formula:C₂₅H₃₂N₃O₆P*2Na
Molecular Weight:547.499
Hs Code.:

Synonyms:N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

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Chemical Property of N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

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Technology Process of N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

There total 5 articles about N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96914-84-0
C₃₉H₄₆N₃O₆P

: 96948-40-2
N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; water; for 1.5h; under 760 Torr;
DOI:10.1021/jm00147a015

Reference yield:

: 74193-68-3
N-tert-butyloxycarbonyl-L-phenylalanyl-L-leucine benzyl ester

: 96948-40-2
N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / trifluoroacetic acid / 1.5 h / Ambient temperature

2: Et₃N / tetrahydrofuran; CH₂Cl₂ / 2 h / Ambient temperature

3: 58 percent / 1N methanolic hydrazine / 72 h / Ambient temperature

4: 50 percent / pyridine / CH₂Cl₂ / 17 h / Ambient temperature

5: H₂, NaHCO₃ / 10percent Pd/C / ethanol; H₂O / 1.5 h / 760 Torr

With pyridine; hydrogen; sodium hydrogencarbonate; triethylamine; trifluoroacetic acid; hydrazine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00147a015

Reference yield:

: 73994-87-3
(S)-benzyl 2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanoate hydrochloride

: 96948-40-2
N-<<<(3-phenylpropionoyl)amino>methyl>hydroxyphosphinyl>phenylalanylleucine disodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran; CH₂Cl₂ / 2 h / Ambient temperature

2: 58 percent / 1N methanolic hydrazine / 72 h / Ambient temperature

3: 50 percent / pyridine / CH₂Cl₂ / 17 h / Ambient temperature

4: H₂, NaHCO₃ / 10percent Pd/C / ethanol; H₂O / 1.5 h / 760 Torr

With pyridine; hydrogen; sodium hydrogencarbonate; triethylamine; hydrazine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00147a015