O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

Base Information

Chemical Name:O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate
CAS No.:1239325-20-2
Molecular Formula:C₂₆H₃₄N₂O₂
Molecular Weight:406.568
Hs Code.:

Synonyms:O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

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Chemical Property of O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

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Technology Process of O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

There total 4 articles about O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1239325-66-6
1-benzyl-3,3-dimethylindolin-5-yl 4-nitrophenylcarbonate

: 161353-93-1
1-cyclohexyl-N-methylmethanamine hydrochloride

: 1239325-20-2
O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

Guidance literature:: With triethylamine; In acetonitrile; for 1h; Cooling with ice;

Reference yield:

: 1239325-65-5
tert-butyl N-(cyclohexylmethyl)-N-methylcarbamate

: 1239325-20-2
O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

2: triethylamine / acetonitrile / 1 h / Cooling with ice

With hydrogenchloride; triethylamine; In ethyl acetate; acetonitrile;

Reference yield:

: 3218-02-8
cyclohexylmethylamine

: 1239325-20-2
O-(1-benzyl-3,3-dimethyl indolin-5-yl)-N-(cyclohexylmethyl)-N-methyl carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 1 h / Cooling with ice

2: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice

3: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

4: triethylamine / acetonitrile / 1 h / Cooling with ice

With hydrogenchloride; sodium hydride; triethylamine; In tetrahydrofuran; ethyl acetate; acetonitrile; mineral oil;