benzaldehyde benzyl(1-benzyl-5-chloro-6-oxo-1,6-dihydro-4-pyridazinyl)hydrazone

Base Information

Chemical Name:benzaldehyde benzyl(1-benzyl-5-chloro-6-oxo-1,6-dihydro-4-pyridazinyl)hydrazone
CAS No.:59026-52-7
Molecular Formula:C₂₅H₂₁ClN₄O
Molecular Weight:428.921
Hs Code.:
Mol file:59026-52-7.mol

Synonyms:2-Benzyl-5-{N-benzyl-N'-[1-phenyl-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzaldehyde benzyl(1-benzyl-5-chloro-6-oxo-1,6-dihydro-4-pyridazinyl)hydrazone

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Technology Process of benzaldehyde benzyl(1-benzyl-5-chloro-6-oxo-1,6-dihydro-4-pyridazinyl)hydrazone

There total 2 articles about benzaldehyde benzyl(1-benzyl-5-chloro-6-oxo-1,6-dihydro-4-pyridazinyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 100-44-7
benzyl chloride

: 91063-66-0
5-benzylidene-hydrazino-4-chloro-3(2H)-pyridazinone

: 59026-52-7
2-Benzyl-5-{N-benzyl-N'-[1-phenyl-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570210501

Reference yield:

: 100-52-7
benzaldehyde

: 59026-52-7
2-Benzyl-5-{N-benzyl-N'-[1-phenyl-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ethanol / 2 h / Heating

2: 59 percent / anhydrous K₂CO₃ / dimethylformamide / 3 h / 70 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210501

Reference yield:

: 59026-52-7
2-Benzyl-5-{N-benzyl-N'-[1-phenyl-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

: 90330-88-4
3-phenyl-1H-pyrazolo<3,4-d>pyridazin-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 5 h / Irradiation

2: 80 percent / AlCl₃ / toluene / 3 h / 50 °C

With aluminium trichloride; In toluene; benzene;