1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten

Base Information

• Chemical Name: 1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten
• CAS No.: 105141-08-0
• Molecular Formula: C₃₂H₃₃ClN₂O
• Molecular Weight: 497.08

Synonyms:1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten

Chemical Property of 1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten

Chemical Property:

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Technology Process of 1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten

There total 1 articles about 1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-pyrrolidinocyclopent-1-ene (7148-07-4) + N-p-chlorophenyltriphenylphosphinimine (31641-65-3) + 2-diazo-1,3-bis(4-methylphenyl)propane-1,3-dione (105141-03-5) → 1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten (105141-08-0)

Guidance literature:

Yield given. Multistep reaction; 1.) xylene, 30 min, 100 deg C, 2.) xylene, 3 h, RT;

Reference yield: 84.0%

1-<1-(4-Chlorphenylimino)-3-hydroxy-2,3-bis(4-methylphenyl)-2-propenyl>-2-pyrrolidino-1-cyclopenten (105141-08-0) → 4-(4-Chlorphenylimino)-4,5,6,7-tetrahydro-2,3-bis(4-methylphenyl)cyclopentapyran (105141-10-4)

Guidance literature:

With sulfuric acid; In ethanol; for 15h;

upstream raw materials:

1-pyrrolidinocyclopent-1-ene

N-p-chlorophenyltriphenylphosphinimine

2-diazo-1,3-bis(4-methylphenyl)propane-1,3-dione

Downstream raw materials:

4-(4-Chlorphenylimino)-4,5,6,7-tetrahydro-2,3-bis(4-methylphenyl)cyclopentapyran

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