tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

Base Information

Chemical Name:tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate
CAS No.:1422385-92-9
Molecular Formula:C₁₃H₁₂ClF₂N₃O₂
Molecular Weight:315.707
Hs Code.:

Synonyms:tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

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Chemical Property of tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

Chemical Property:

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Technology Process of tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

There total 5 articles about tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13831-03-3
tert-butyl prop-2-ynoate

: 1422386-25-1
2-azido-4-chloro-1,3-difluorobenzene

: 1422385-92-9
tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: With copper diacetate; potassium carbonate; In dimethyl sulfoxide; at 20 ℃;

Reference yield:

: 287172-82-1
3-chloro-2,6-difluoroaniline

: 1422385-92-9
tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; trifluoroacetic acid / water / 0.5 h / 0 °C

1.2: 0 °C

2.1: copper diacetate; potassium carbonate / dimethyl sulfoxide / 20 °C

With copper diacetate; potassium carbonate; trifluoroacetic acid; sodium nitrite; In water; dimethyl sulfoxide;

Reference yield:

: 870606-47-6
C₁₁H₁₂ClF₂NO₂

: 1422385-92-9
tert-butyl 1-(3-chloro-2,6-difluorophenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

1.2: 0 °C

2.1: copper diacetate; potassium carbonate / dimethyl sulfoxide / 20 °C

With copper diacetate; potassium carbonate; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;