L-hydroxyproline-fenofibric acid ester hydrochloride

Base Information

Chemical Name:L-hydroxyproline-fenofibric acid ester hydrochloride
CAS No.:852056-09-8
Molecular Formula:C₂₂H₂₂ClNO₆*ClH
Molecular Weight:468.334
Hs Code.:

Synonyms:L-hydroxyproline-fenofibric acid ester hydrochloride

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Chemical Property of L-hydroxyproline-fenofibric acid ester hydrochloride

Chemical Property:

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Technology Process of L-hydroxyproline-fenofibric acid ester hydrochloride

There total 3 articles about L-hydroxyproline-fenofibric acid ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 852056-06-5
C₃₁H₃₈ClNO₈

: 852056-09-8
L-hydroxyproline-fenofibric acid ester hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; In dichloromethane; at 5 ℃; for 96h;

Reference yield:

: 42019-78-3
4-chloro-4'-hydroxybenzophenone

: 852056-09-8
L-hydroxyproline-fenofibric acid ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / 2 h / Heating / reflux

1.2: 8 h / Heating / reflux

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 96 h / 20 °C

3.1: hydrogenchloride; acetic acid / dichloromethane / 96 h / 5 °C

With hydrogenchloride; dmap; sodium hydroxide; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

Reference yield:

: 42017-89-0
fenofibric acid

: 170850-75-6
BOC-Hyp-OtBu

: 852056-09-8
L-hydroxyproline-fenofibric acid ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 96 h / 20 °C

2: hydrogenchloride; acetic acid / dichloromethane / 96 h / 5 °C

With hydrogenchloride; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;