2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

Base Information

Chemical Name:2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate
CAS No.:652169-56-7
Molecular Formula:C₂₁H₂₆O₇S
Molecular Weight:422.499
Hs Code.:

Synonyms:2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

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Chemical Property of 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

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Technology Process of 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

There total 1 articles about 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 124-63-0
methanesulfonyl chloride

: 221675-77-0
2,4-dimethoxybenzyl 3-hydroxy-2,2-dimethyldihydrocinnamate

: 652169-56-7
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ol036052l

Reference yield:

: 652169-56-7
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

: 768-49-0
β,β-dimethyl styrene radical cation

Guidance literature:: Multi-step reaction with 3 steps

1: ceric ammonium nitrate / H₂O; acetonitrile / 1 h / 20 °C

2: 0.264 g / tributylphosphine / CH₂Cl₂ / 2 h / 20 °C

3: various solvent(s); 2,2,2-trifluoro-ethanol / Photolysis

With ammonium cerium(IV) nitrate; tributylphosphine; In dichloromethane; 2,2,2-trifluoroethanol; water; acetonitrile;
DOI:10.1021/ol036052l

Reference yield:

: 652169-56-7
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2,2-dimethyl-3-phenylpropanoate

: 652169-55-6
3-methanesulfonyloxy-2,2-dimethyl-3-phenyl-propionic acid 2-thioxo-2H-pyridin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: ceric ammonium nitrate / H₂O; acetonitrile / 1 h / 20 °C

2: 0.264 g / tributylphosphine / CH₂Cl₂ / 2 h / 20 °C

With ammonium cerium(IV) nitrate; tributylphosphine; In dichloromethane; water; acetonitrile;
DOI:10.1021/ol036052l