methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

Base Information

Chemical Name:methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate
CAS No.:1544664-52-9
Molecular Formula:C₂₀H₁₉F₆NO₂
Molecular Weight:419.367
Hs Code.:

Synonyms:methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

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Chemical Property of methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

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Technology Process of methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

There total 4 articles about methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 1544664-48-3
methyl 5-iodo-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

: 1544664-52-9
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Inert atmosphere;

Reference yield:

: 75091-99-5
4-(trifluoromethyl)cyclohexan-1-one

: 1544664-52-9
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 h / 90 °C

2: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 4 h / 20 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; N-iodo-succinimide; copper(l) iodide; sodium tris(acetoxy)borohydride; acetic acid; trifluoroacetic acid; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 5159-59-1
methyl 6-amino-2-naphthoate

: 1544664-52-9
methyl 5-(trifluoromethyl)-6-((cis-4-(trifluoromethyl)cyclohexyl)amino)-2-naphthoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 h / 90 °C

2: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 4 h / 20 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; N-iodo-succinimide; copper(l) iodide; sodium tris(acetoxy)borohydride; acetic acid; trifluoroacetic acid; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;