4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide

Base Information

• Chemical Name: 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide
• CAS No.: 83049-90-5
• Molecular Formula: C₃₃H₄₄O₅
• Molecular Weight: 520.709

Synonyms:4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide

Chemical Property of 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide

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Technology Process of 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide

There total 1 articles about 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

methylmagnesium bromide (75-16-1) + 1-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4-<1-methyl-1-(1-methyl-1-p-acetylphenylethylperoxy)ethyl>benzene (79506-38-0) → 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide (83049-90-5)

Guidance literature:

In diethyl ether; at 0 - 5 ℃; for 2h;

Reference yield: 76.0%

tert-amyl hydroperoxide (3425-61-4) + 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide (83049-90-5) → 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-<1-methyl-1-(1,1-dimethylpropylperoxy)ethyl>-di-(1-methyl-1-phenylethyl) peroxide (83049-92-7)

Guidance literature:

With perchloric acid; In acetic acid; at 20 ℃; for 3h;

Reference yield: 72.0%

4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1-hydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide (83049-90-5) → 4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-isopropenyl-di-(1-methyl-1-phenylethyl) peroxide (83049-94-9)

Guidance literature:

With iodine; In acetic acid; at 80 ℃; for 2.5h;

upstream raw materials:

methylmagnesium bromide

1-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4-<1-methyl-1-(1-methyl-1-p-acetylphenylethylperoxy)ethyl>benzene

Downstream raw materials:

4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-<1-methyl-1-(1,1-dimethylpropylperoxy)ethyl>-di-(1-methyl-1-phenylethyl) peroxide

4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-isopropenyl-di-(1-methyl-1-phenylethyl) peroxide

4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>-4'-(1-methyl-1,2-dihydroxyethyl)-di-(1-methyl-1-phenylethyl) peroxide

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