5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Base Information

Chemical Name:5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate
CAS No.:1434878-90-6
Molecular Formula:C₂₁H₂₀O₆
Molecular Weight:368.386
Hs Code.:

Synonyms:5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Suppliers and Price of 5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

There total 2 articles about 5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1434878-81-5
3-(2,6-dihydroxy-4-isopropylphenyl)isobenzofuran-1(3H)-one

: 108-24-7
acetic anhydride

: 1434878-90-6
5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Guidance literature:: With dmap; In chloroform; at 20 ℃; for 12h;
DOI:10.3390/molecules18021881

Reference yield:

: 16859-59-9
3-hydroxy-1(3H)-isobenzofuranone

: 1434878-90-6
5-isopropyl-2-(3-oxo-1,3-dihydroisobenzofuran-1-yl)-1,3-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h / 20 °C

1.2: 7 h / Reflux

2.1: acetic acid; mercury(II) diacetate; sodium acetate / 5 h / Reflux

2.2: 0.25 h

3.1: dmap / chloroform / 12 h / 20 °C

With dmap; mercury(II) diacetate; sodium acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; acetonitrile;
DOI:10.3390/molecules18021881