1,8-naphthylene phenylboronate

Base Information

• Chemical Name: 1,8-naphthylene phenylboronate
• CAS No.: 60548-84-7
• Molecular Formula: C₁₆H₁₁BO₂
• Molecular Weight: 246.073

Synonyms:1,8-naphthylene phenylboronate

Chemical Property of 1,8-naphthylene phenylboronate

Chemical Property:

Purity/Quality:

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Technology Process of 1,8-naphthylene phenylboronate

There total 6 articles about 1,8-naphthylene phenylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,8-dihydroxynaphthalene (569-42-6) + phenylboronic acid (98-80-6) → 1,8-naphthylene phenylboronate (60548-84-7)

Guidance literature:

In acetonitrile; Heating;

DOI:10.1039/d0dt00745e

Reference yield:

1,8-dihydroxynaphthalene (569-42-6) + 2-phenyl-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine (24341-81-9) → 1,8-naphthylene phenylboronate (60548-84-7) + naphthalene-1,8-diamine (479-27-6)

Guidance literature:

In chloroform-d1; at 50 ℃; for 96h;

DOI:10.1039/d0dt00745e

Reference yield:

1,8-dihydroxynaphthalene (569-42-6) + 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole (24388-23-6) → 2,3-dimethyl-2,3-butane diol (76-09-5) + 1,8-naphthylene phenylboronate (60548-84-7)

Guidance literature:

In chloroform-d1; at 50 ℃; for 24h;

DOI:10.1039/d0dt00745e

upstream raw materials:

1,8-dihydroxynaphthalene

phenylboronic acid

2-phenyl-1,3,2-benzodioxaborole

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

Downstream raw materials:

1,8-dihydroxynaphthalene

phenylboronic acid

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