6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)

Base Information

Chemical Name:6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)
CAS No.:92584-67-3
Molecular Formula:BrH*C₁₃H₁₆N₂O₂
Molecular Weight:313.194
Hs Code.:
DSSTox Substance ID:DTXSID20919089

Synonyms:92584-67-3;DTXSID20919089;6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)

Suppliers and Price of 6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)

Chemical Property:

Vapor Pressure:5.76E-06mmHg at 25°C
Boiling Point:379.7°Cat760mmHg
Flash Point:183.4°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:312.04734
Heavy Atom Count:18
Complexity:304

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)CCNC3CC3)OC1=O.Br

Technology Process of 6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1)

There total 2 articles about 6-[2-(Cyclopropylamino)ethyl]-3-methyl-1,3-benzoxazol-2(3H)-one--hydrogen bromide (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 92584-73-1
3-methyl-6-(2-bromoethyl)-benzoxazolinone

: 765-30-0
Cyclopropylamine

: 92584-67-3
methyl-3 (cyclopropylamino-2 ethyl)-6 benzoxazolinone bromhydrate

Guidance literature:: In 1,4-dioxane; for 15h; Heating;

Reference yield:

: 79851-85-7
6-(2-bromoacetyl)-3-methylbenzo[d]oxazol-2(3H)-one

: 92584-67-3
methyl-3 (cyclopropylamino-2 ethyl)-6 benzoxazolinone bromhydrate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylsilane, trifluoroacetic acid

2: 80 percent / dioxane / 15 h / Heating

With triethylsilane; trifluoroacetic acid; In 1,4-dioxane;