4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

Base Information

Chemical Name:4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]
CAS No.:1270020-08-0
Molecular Formula:C₁₇H₂₀ClN₇O₂S₂
Molecular Weight:453.977
Hs Code.:

Synonyms:4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

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Technology Process of 4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

There total 2 articles about 4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 35929-79-4
4-(4-chloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

: 79-19-6
thiosemicarbazide

: 1270020-08-0
4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

Guidance literature:: In methanol; dimethyl sulfoxide; for 10h; Reflux;
DOI:10.1016/j.ejmech.2010.12.006

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1270020-08-0
4-(4-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3,5-bis[2-(aminothioxomethyl)hydrazide]

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / methanol / 4 h / Reflux

2: methanol; dimethyl sulfoxide / 10 h / Reflux

With ammonium hydroxide; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2010.12.006