C₂₂H₂₅ClN₆O₃S

Base Information

Chemical Name:C₂₂H₂₅ClN₆O₃S
CAS No.:1353623-28-5
Molecular Formula:C₂₂H₂₅ClN₆O₃S
Molecular Weight:488.998
Hs Code.:

C<sub>22</sub>H<sub>25</sub>ClN<sub>6</sub>O<sub>3</sub>S

Synonyms:C₂₂H₂₅ClN₆O₃S

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Chemical Property of C₂₂H₂₅ClN₆O₃S

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Technology Process of C₂₂H₂₅ClN₆O₃S

There total 10 articles about C₂₂H₂₅ClN₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₉N₅

: 89979-12-4
5-chloro-2-(methylsulfonamido)benzoic acid

: 1353623-28-5
C₂₂H₂₅ClN₆O₃S

Guidance literature:: 5-chloro-2-(methylsulfonamido)benzoic acid; With HATU; In N,N-dimethyl-formamide; for 1h;

C₁₄H₁₉N₅; With triethylamine; In N,N-dimethyl-formamide; for 16h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353623-28-5
C₂₂H₂₅ClN₆O₃S

Guidance literature:: Multi-step reaction with 9 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: sodium ethanolate / ethanol / 3 h / 90 °C

5.1: hydrogenchloride / 1,4-dioxane / 1 h

5.2: 2 h

6.1: pyridine / dichloromethane / 1.5 h / Inert atmosphere

7.1: tetrahydrofuran / 2 h / 70 °C

8.1: hydrogen / palladium on activated charcoal / methanol / 1 h

9.1: HATU / N,N-dimethyl-formamide / 1 h

9.2: 16 h

With pyridine; hydrogenchloride; sodium bis(trimethylsilyl)amide; hydrogen; sodium ethanolate; hydrazinium monoacetate; caesium carbonate; HATU; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 200184-53-8
(S)-1-tert-butyl 2-methyl piperidine-1,2-dicarboxylate

: 1353623-28-5
C₂₂H₂₅ClN₆O₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

1.2: -78 - -40 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium ethanolate / ethanol / 3 h / 90 °C

4.1: hydrogenchloride / 1,4-dioxane / 1 h

4.2: 2 h

5.1: pyridine / dichloromethane / 1.5 h / Inert atmosphere

6.1: tetrahydrofuran / 2 h / 70 °C

7.1: hydrogen / palladium on activated charcoal / methanol / 1 h

8.1: HATU / N,N-dimethyl-formamide / 1 h

8.2: 16 h

With pyridine; hydrogenchloride; sodium bis(trimethylsilyl)amide; hydrogen; sodium ethanolate; hydrazinium monoacetate; HATU; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; ethanol; dichloromethane; N,N-dimethyl-formamide;