4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

Base Information

Chemical Name:4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime
CAS No.:319458-59-8
Molecular Formula:C₁₅H₁₉N₅O₃
Molecular Weight:317.348
Hs Code.:

Synonyms:4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

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Chemical Property of 4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

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Technology Process of 4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

There total 4 articles about 4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 319458-58-7
2,6-diamino-5-[3-(benzyloxy)-1-(nitromethyl)propyl]-4(3H)-pyrimidinone

: 319458-59-8
4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

Guidance literature:: With thiophenol; triethylamine; tin(ll) chloride; In acetonitrile; for 0.5h;
DOI:10.1016/S0040-4039(00)01491-X

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 319458-59-8
4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / NaOH / ethanol / 3 h / 20 °C

2: 90 percent / Et₃N / CH₂Cl₂ / 2.25 h / 0 °C

3: 69 percent / ethyl acetate; H₂O / 50 °C

4: 79 percent / SnCl₂; PhSH; Et₃N / acetonitrile / 0.5 h

With sodium hydroxide; thiophenol; triethylamine; tin(ll) chloride; In ethanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4039(00)01491-X

Reference yield:

: 319458-57-6
(E)-(((4-nitrobut-3-en-1-yl)oxy)methyl)benzene

: 319458-59-8
4-(benzyloxy)-2-(2,4-diamino-6-oxo-1,6-dihydro-5-pyrimidinyl)butanal oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / ethyl acetate; H₂O / 50 °C

2: 79 percent / SnCl₂; PhSH; Et₃N / acetonitrile / 0.5 h

With thiophenol; triethylamine; tin(ll) chloride; In water; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4039(00)01491-X