C₅₄H₆₀O₈

Base Information

Chemical Name:C₅₄H₆₀O₈
CAS No.:83487-67-6
Molecular Formula:C₅₄H₆₀O₈
Molecular Weight:837.066
Hs Code.:

C<sub>54</sub>H<sub>60</sub>O<sub>8</sub>

Synonyms:C₅₄H₆₀O₈

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Chemical Property of C₅₄H₆₀O₈

Chemical Property:

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Technology Process of C₅₄H₆₀O₈

There total 14 articles about C₅₄H₆₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83511-07-3
3,7-dihydroxy-2-naphthoic acid

: 83487-67-6
C₅₄H₆₀O₈

Guidance literature:: Multi-step reaction with 9 steps

1: 52 percent / NaHCO₃ / dimethylformamide / 1 h / 70 °C

2: 80 percent / K₂CO₃ / acetone / 11 h / Heating

3: 1.) n-BuLi, 2.) KOH / 1.) 0 deg C, 1 h; room temperature, overnight, 2.) MeOH, reflux, 4 h

4: 99 percent / 4-(dimethylamino)pyridine, cyclohexyl carbodiimide / CH₂Cl₂ / 3 h / Ambient temperature

5: 93 percent / HCl gas / benzene / 0.07 h

6: 87 percent / cupric acetate monohydrate / pyridine / 2.5 h / 40 °C

7: 66 percent / K₂CO₃ / acetone / 45 h / Heating

8: cupric acetate monohydrate / pyridine / 2 h / 42 °C

9: H₂ / Pd/C / ethyl acetate / 1 h

With hydrogenchloride; dmap; potassium hydroxide; n-butyllithium; N-cyclohexylcarbodiimide; hydrogen; copper diacetate; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In pyridine; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/ja00389a050

Reference yield:

: 26513-28-0
sodium 2-carboxy-3-hydroxy-7-naphthalenesulfonate

: 83487-67-6
C₅₄H₆₀O₈

Guidance literature:: Multi-step reaction with 10 steps

1: 81 percent / KOH / 1.5 h / 250 - 300 °C

2: 52 percent / NaHCO₃ / dimethylformamide / 1 h / 70 °C

3: 80 percent / K₂CO₃ / acetone / 11 h / Heating

4: 1.) n-BuLi, 2.) KOH / 1.) 0 deg C, 1 h; room temperature, overnight, 2.) MeOH, reflux, 4 h

5: 99 percent / 4-(dimethylamino)pyridine, cyclohexyl carbodiimide / CH₂Cl₂ / 3 h / Ambient temperature

6: 93 percent / HCl gas / benzene / 0.07 h

7: 87 percent / cupric acetate monohydrate / pyridine / 2.5 h / 40 °C

8: 66 percent / K₂CO₃ / acetone / 45 h / Heating

9: cupric acetate monohydrate / pyridine / 2 h / 42 °C

10: H₂ / Pd/C / ethyl acetate / 1 h

With hydrogenchloride; dmap; potassium hydroxide; n-butyllithium; N-cyclohexylcarbodiimide; hydrogen; copper diacetate; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In pyridine; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/ja00389a050

Reference yield:

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 83487-67-6
C₅₄H₆₀O₈

Guidance literature:: Multi-step reaction with 11 steps

1: 40 percent / H₂SO₄

2: 81 percent / KOH / 1.5 h / 250 - 300 °C

3: 52 percent / NaHCO₃ / dimethylformamide / 1 h / 70 °C

4: 80 percent / K₂CO₃ / acetone / 11 h / Heating

5: 1.) n-BuLi, 2.) KOH / 1.) 0 deg C, 1 h; room temperature, overnight, 2.) MeOH, reflux, 4 h

6: 99 percent / 4-(dimethylamino)pyridine, cyclohexyl carbodiimide / CH₂Cl₂ / 3 h / Ambient temperature

7: 93 percent / HCl gas / benzene / 0.07 h

8: 87 percent / cupric acetate monohydrate / pyridine / 2.5 h / 40 °C

9: 66 percent / K₂CO₃ / acetone / 45 h / Heating

10: cupric acetate monohydrate / pyridine / 2 h / 42 °C

11: H₂ / Pd/C / ethyl acetate / 1 h

With hydrogenchloride; dmap; potassium hydroxide; n-butyllithium; sulfuric acid; N-cyclohexylcarbodiimide; hydrogen; copper diacetate; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In pyridine; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/ja00389a050