1-Nitro-3-(1-azidoethyl)benzene

Base Information

Chemical Name:1-Nitro-3-(1-azidoethyl)benzene
CAS No.:246240-16-4
Molecular Formula:C₈H₈N₄O₂
Molecular Weight:192.177
Hs Code.:
DSSTox Substance ID:DTXSID901304810

Synonyms:1-(1-azidoethyl)-3-nitrobenzene;246240-16-4;1-Nitro-3-(1-azidoethyl)benzene;OJMDFRMRSPQROO-UHFFFAOYSA-N;DTXSID901304810;DB-131347

Suppliers and Price of 1-Nitro-3-(1-azidoethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Nitro-3-(1-azidoethyl)benzene

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:192.06472551
Heavy Atom Count:14
Complexity:257

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=CC(=CC=C1)[N+](=O)[O-])N=[N+]=[N-]

Technology Process of 1-Nitro-3-(1-azidoethyl)benzene

There total 3 articles about 1-Nitro-3-(1-azidoethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 5400-78-2
1-(3-nitrophenyl)ethanol

: 246240-16-4
1-(1-azidoethyl)-3-nitrobenzene

Guidance literature:: With N-methylimidazolium tetrafluoroborate; sodium azide; at 100 ℃; for 8h; Green chemistry;
DOI:10.1002/jccs.201400046

Reference yield:

: O-Methanesulfonyl-1-nitro-3-(1-hydroxyethyl)benzene

: 246240-16-4
1-(1-azidoethyl)-3-nitrobenzene

Guidance literature:: In dimethyl sulfoxide;

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 246240-16-4
1-(1-azidoethyl)-3-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

2: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / Inert atmosphere

With sodium tetrahydroborate; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; toluene;
DOI:10.3109/14756366.2013.793184