(3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

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Chemical Name:(3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone
CAS No.:1201359-25-2
Molecular Formula:C₁₅H₂₄F₃NO₄Si
Molecular Weight:367.441
Hs Code.:

Synonyms:(3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

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Chemical Property of (3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

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Technology Process of (3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

There total 2 articles about (3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1201359-63-8
(1'S,3R,4R)-4-acetoxy-3-(1'-trimethylsilyloxy-2',2',2'-trifluoroethyl)-2-azetidinone

: 173459-91-1
(S)-6-methoxy-1-(trimethylsilyloxy)cyclohex-1-ene

: C₁₅H₂₄F₃NO₄Si

: 1201359-25-2
(3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

Guidance literature:: (S)-6-methoxy-1-(trimethylsilyloxy)cyclohex-1-ene; With methyllithium; In tetrahydrofuran; diethyl ether; at -60 - 0 ℃; for 0.833333h;

(1'S,3R,4R)-4-acetoxy-3-(1'-trimethylsilyloxy-2',2',2'-trifluoroethyl)-2-azetidinone; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h;

Reference yield: 50.0%

: 1201359-60-5
(1'S,3R,4R)-4-acetoxy-3-(1'-trimethylsilyloxy-2',2',2'-trifluoroethyl)-1-(trimethylsilyl)-2-azetidinone

: 173459-91-1
(S)-6-methoxy-1-(trimethylsilyloxy)cyclohex-1-ene

: C₁₅H₂₄F₃NO₄Si

: 1201359-25-2
(3S,4R)-4-[(1R,3S)-3-methoxy-2-oxo-cyclohexyl]-3-[1-(S)-trimethylsilyloxy-2,2,2-trifluoroethyl]-2-azetidinone

Guidance literature:: (S)-6-methoxy-1-(trimethylsilyloxy)cyclohex-1-ene; With methyllithium; In tetrahydrofuran; diethyl ether; at -60 - 0 ℃; for 0.833333h;

(1'S,3R,4R)-4-acetoxy-3-(1'-trimethylsilyloxy-2',2',2'-trifluoroethyl)-1-(trimethylsilyl)-2-azetidinone; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h;