Technology Process of C20H19F2N7O
There total 7 articles about C20H19F2N7O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H19F2N5O*ClH;
With
toluene-4-sulfonic acid; triethylamine; {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride};
In
toluene;
for 216h;
Reflux;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonia; dihydrogen peroxide / ethanol; water / 2.17 h / 20 °C
2: pyridine / dmap / toluene / 24 h / 20 °C / Inert atmosphere
3: sodium hydride; methanol / toluene; mineral oil / 7 h / 65 °C
4: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / ethanol; water / 1 h / 775.74 Torr
5: toluene-4-sulfonic acid; triethylamine; {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride} / toluene / 216 h / Reflux
With
pyridine; hydrogenchloride; methanol; ammonia; hydrogen; dihydrogen peroxide; sodium hydride; toluene-4-sulfonic acid; triethylamine; {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride};
dmap; 5%-palladium/activated carbon;
In
ethanol; water; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dmap / toluene / 24 h / 20 °C / Inert atmosphere
2: sodium hydride; methanol / toluene; mineral oil / 7 h / 65 °C
3: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / ethanol; water / 1 h / 775.74 Torr
4: toluene-4-sulfonic acid; triethylamine; {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride} / toluene / 216 h / Reflux
With
pyridine; hydrogenchloride; methanol; hydrogen; sodium hydride; toluene-4-sulfonic acid; triethylamine; {N'-[(dimethylamino)methylene]-N,N-dimethylhydrazonoformamide dihydrochloride};
dmap; 5%-palladium/activated carbon;
In
ethanol; water; toluene; mineral oil;