2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside
CAS No.:917568-50-4
Molecular Formula:C₃₂H₅₂O₇Si₂
Molecular Weight:604.932
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Suppliers and Price of 2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

There total 6 articles about 2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 917568-49-1
2-(trimethylsilyl)ethyl 2-O-benzyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 917568-50-4
2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 8h;
DOI:10.1021/ja065907x

Reference yield:

: 848647-23-4
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

: 917568-50-4
2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / NaH / dimethylformamide / 1.5 h / 0 °C

2: 90 percent / p-toluenesulfonic acid monohydrate / methanol / 2 h

3: 96 percent / imidazole / dimethylformamide / 8 h

With 1H-imidazole; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja065907x

Reference yield:

: 117252-95-6
2-(trimethylsilyl)ethyl β-D-galactopyranoside

: 917568-50-4
2-(trimethylsilyl)ethyl 2-O-benzyl-6-O-tert-butyldimethysilyl-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: dibutyltin oxide / methanol; toluene / 3.5 h / Heating

1.2: 97 percent / tetrabutylammonium bromide / benzene / 1 h / Heating

2.1: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 3 h / 55 °C

3.1: 82 percent / NaH / dimethylformamide / 1.5 h / 0 °C

4.1: 90 percent / p-toluenesulfonic acid monohydrate / methanol / 2 h

5.1: 96 percent / imidazole / dimethylformamide / 8 h

With 1H-imidazole; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja065907x