4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

Base Information

Chemical Name:4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol
CAS No.:608140-30-3
Molecular Formula:C₁₅H₁₃Cl₂N₅S
Molecular Weight:366.274
Hs Code.:

Synonyms:4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

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Chemical Property of 4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

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Technology Process of 4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

There total 3 articles about 4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75-15-0,12122-00-8
carbon disulfide

: 133239-50-6
N-amino-2-{2'-[(2'',6''-dichlorophenyl)amino]phenyl}acetamide

: 608140-30-3
4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

Guidance literature:: carbon disulfide; N-amino-2-{2'-[(2'',6''-dichlorophenyl)amino]phenyl}acetamide; With potassium hydroxide; for 6h; Reflux;

With hydrazine hydrate; for 6h; Reflux;
DOI:10.1016/j.ejmech.2014.07.051

Reference yield:

: 15307-86-5
[2-(2,6-dichloroanilino)phenyl]acetic acid

: 608140-30-3
4-amino-5-({2'-[(2'',6''-dichlorophenyl)amino]phenyl}methyl)-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride

2: carbon disulfide; potassium hydroxide

3: hydrazine hydrate

With carbon disulfide; thionyl chloride; hydrazine hydrate; potassium hydroxide;