Technology Process of C20H23NO2S
There total 5 articles about C20H23NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine;
In
toluene;
at 120 ℃;
for 10h;
Inert atmosphere;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 80 °C
3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
4: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine / toluene / 10 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; di-isopropyl azodicarboxylate; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
1: Mitsunobu reaction;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C
2: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine / toluene / 10 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; potassium carbonate; triethylamine;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja201204g
