hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Base Information

Chemical Name:hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside
CAS No.:924295-29-4
Molecular Formula:C₄₁H₆₃NO₆
Molecular Weight:665.954
Hs Code.:

Synonyms:hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

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Technology Process of hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

There total 1 articles about hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: pent-4-enoic acid (2-hexadecyloxy-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl)-amide

: 924295-29-4
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Guidance literature:: With methanol; toluene-4-sulfonic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/jm0611556

Reference yield: 87.0%

: 924295-29-4
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 215302-04-8
9-(4-Methoxy-phenyl)-2,4,8,10-tetraoxa-3-thia-spiro[5.5]undecane 3,3-dioxide

: C₅₄H₇₈NO₁₃S^(1-)*Na⁽¹⁺⁾

Guidance literature:: hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

9-(4-Methoxy-phenyl)-2,4,8,10-tetraoxa-3-thia-spiro[5.5]undecane 3,3-dioxide; In tetrahydrofuran; N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1021/jm0611556

Reference yield:

: 924295-29-4
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 23737-51-1,7305-59-1
solketal tosylate

: 924295-64-7
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2,2-dimethyl-1,3-dioxolan-4(R)-ylmethyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 924295-65-8
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2,2-dimethyl-1,3-dioxolan-4(S)-ylmethyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Guidance literature:: hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

solketal tosylate; In N,N-dimethyl-formamide; at 90 ℃; for 0.5h;
DOI:10.1021/jm0611556