hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Base Information

Chemical Name:hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside
CAS No.:924295-66-9
Molecular Formula:C₄₄H₆₉NO₈
Molecular Weight:740.034
Hs Code.:

Synonyms:hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

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Chemical Property of hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

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Technology Process of hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

There total 3 articles about hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 924295-64-7
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2,2-dimethyl-1,3-dioxolan-4(R)-ylmethyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 924295-66-9
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In methanol; at 20 ℃;
DOI:10.1021/jm0611556

Reference yield:

: hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2,2-dimethyl-1,3-dioxolan-4(R,S)-ylmethyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 924295-66-9
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 924295-67-0
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(S),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In methanol; at 20 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/jm0611556

Reference yield:

: 924295-29-4
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-2-N-(pent-4-enoyl)-α-D-glucopyranoside

: 924295-66-9
hexadecyl 2-amino-3,4-di-O-benzyl-2-deoxy-6-O-(2(R),3-dihydroxypropyl)-2-N-(pent-4-enoyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.17 h

1.2: 150 mg / dimethylformamide / 0.5 h / 90 °C

2.1: trifluoroacetic acid / methanol / 20 °C

With sodium hydride; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0611556