(S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

Base Information

Chemical Name:(S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide
CAS No.:1092380-93-2
Molecular Formula:C₁₇H₂₀N₂O
Molecular Weight:268.359
Hs Code.:

Synonyms:(S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

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Technology Process of (S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

There total 2 articles about (S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 75-30-9
2-iodo-propane

: 14850-88-5,14850-89-6,956-07-0
benzoylhydrazone of benzaldehyde

: 1092380-93-2
(S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

Guidance literature:: With air; triethyl borane; C₂₆H₃₀N₂O*F₆P^(1-)*H⁽¹⁺⁾; diphenylsilane; In hexane; dichloromethane; at -30 ℃; for 4h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja807685r

Reference yield:

: C₁₇H₁₈N₂O

: 1092380-93-2
(S)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

: (R)-N'-(2-methyl-1-phenylpropyl)benzohydrazide

Guidance literature:: With (R,R)-(?)-2,3-bis(t-butylmethylphosphino)quinoxaline; hydrogen; nickel(II) acetate tetrahydrate; acetic acid; In 2,2,2-trifluoroethanol; at 50 ℃; for 24h; under 22502.3 Torr; Overall yield = 99 percent; Overall yield = 53.1 mg; enantioselective reaction; Autoclave; Schlenk technique;
DOI:10.1002/ejoc.202100642