6-dodecyl-2-methoxy-1,4-benzoquinone

Base Information

• Chemical Name: 6-dodecyl-2-methoxy-1,4-benzoquinone
• CAS No.: 4075-01-8
• Molecular Formula: C19H30 O3
• Molecular Weight: 306.445
• Hs Code.: 2914690090
• Mol file: 4075-01-8.mol

Synonyms:p-Benzoquinone,2-dodecyl-6-methoxy- (7CI,8CI); 6-Dodecyl-2-methoxy-1,4-benzoquinone

Chemical Property of 6-dodecyl-2-methoxy-1,4-benzoquinone

Chemical Property:

• Vapor Pressure: 3.24E-07mmHg at 25°C
• Boiling Point: 418.6°Cat760mmHg
• Flash Point: 180.3°C
• PSA: 43.37000
• Density: 0.99g/cm³
• LogP: 4.90590

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-dodecyl-2-methoxy-1,4-benzoquinone

There total 4 articles about 6-dodecyl-2-methoxy-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

2-Dodecyl-6-methoxy-phenol (148173-55-1) → 2-dodecyl-6-methoxycyclohexa-2,5-diene-1, 4-dione (4075-01-8)

Guidance literature:

With potassium nitrososulfonate; borate buffer pH 9; In ethanol; water; for 5h;

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) → 2-dodecyl-6-methoxycyclohexa-2,5-diene-1, 4-dione (4075-01-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) Mg / 1.) Et₂O, reflux, 30 min 2.) THF, rt, overnight

2: 76 percent / H₂ / 10percent Pd/C / ethanol

3: 4 percent / borate buffer pH 9, potassium nitrosodisulfonate (Fremy-salt) / ethanol; H₂O / 5 h

With potassium nitrososulfonate; borate buffer pH 9; hydrogen; magnesium; palladium on activated charcoal; In ethanol; water;

Reference yield:

2-(1-Hydroxy-dodecyl)-6-methoxy-phenol → 2-dodecyl-6-methoxycyclohexa-2,5-diene-1, 4-dione (4075-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / H₂ / 10percent Pd/C / ethanol

2: 4 percent / borate buffer pH 9, potassium nitrosodisulfonate (Fremy-salt) / ethanol; H₂O / 5 h

With potassium nitrososulfonate; borate buffer pH 9; hydrogen; palladium on activated charcoal; In ethanol; water;

upstream raw materials:

1-dodecyl-3,5-dimethoxy-benzene

2-Dodecyl-6-methoxy-phenol

3-methoxy-2-hydroxybenzaldehyde

Refernces