13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

Base Information

Chemical Name:13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide
CAS No.:877285-47-7
Molecular Formula:C₃₂H₃₂BrN₅O₃S
Molecular Weight:646.608
Hs Code.:

Synonyms:13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

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Chemical Property of 13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

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Technology Process of 13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

There total 1 articles about 13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 863567-20-8
13-cyclohexyl-6-oxo-6,7-dihydro-5H-indolo[2,1-d][1,4]benzodiazepine-10-carboxylic acid

: 877285-33-1
1-amino-N-(5-bromothiazol-2-yl)cyclopentanecarboxamide

: 877285-47-7
13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

Guidance literature:: 13-cyclohexyl-6-oxo-6,7-dihydro-5H-indolo[2,1-d][1,4]benzodiazepine-10-carboxylic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); at 22 ℃; for 0.25h;

1-amino-N-(5-bromothiazol-2-yl)cyclopentanecarboxamide; In DMF (N,N-dimethyl-formamide); at 22 ℃; for 18h;

Reference yield: 62.0%

: 877285-47-7
13-cyclohexyl-6,7-dihydro-6-oxo-N-[(1-((5-bromothiazol-2-yl)carbamoyl)cyclopentyl)]-5H-indolo[1,2-d][1,4]benzodiazepine-10-carboxamide

: 14047-29-1
4-carboxyphenylboronic acid

: 4-[2-[[[1-[[(13-cyclohexyl-6,7-dihydro-6-oxo-5H-indolo[1,2-d][1,4]benzodiazepin-10-yl)carbonyl]amino]cyclopentyl]carbonyl]amino]-5-thiazolyl]-benzoic acid

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 130 ℃; for 0.0833333h; microwave;