3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

Base Information

Chemical Name:3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate
CAS No.:1345964-75-1
Molecular Formula:C₂F₃O₂*C₂₂H₂₁N₂O
Molecular Weight:442.438
Hs Code.:

Synonyms:3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

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Chemical Property of 3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

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Technology Process of 3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

There total 6 articles about 3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1345964-73-9
(2-methylimidazo[1,2-a]pyridin-3-yl)diphenylmethanol

: 77-78-1
dimethyl sulfate

: 76-05-1
trifluoroacetic acid

: 1345964-75-1
3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

Guidance literature:: (2-methylimidazo[1,2-a]pyridin-3-yl)diphenylmethanol; dimethyl sulfate; In 1,4-dioxane; Inert atmosphere; Sealed tube;

trifluoroacetic acid;
DOI:10.1021/jm400904m

Reference yield:

: 92351-15-0
2-amino-1-(prop-2-yn-1-yl)pyridin-1-ium bromide

: 1345964-75-1
3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; triethylamine / N,N-dimethyl-formamide

2.1: N-Bromosuccinimide / Inert atmosphere

3.1: TurboGrignard / tetrahydrofuran / -15 - 10 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: 1,4-dioxane / Inert atmosphere; Sealed tube

With N-Bromosuccinimide; copper(l) iodide; TurboGrignard; triethylamine; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm400904m

Reference yield:

: 934-37-2
2-methylimidazo[1,2-a]pyridine

: 1345964-75-1
3-(hydroxydiphenylmethyl)-1,2-dimethylimidazo[1,2-a]-pyridin-1-ium trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / Inert atmosphere

2.1: TurboGrignard / tetrahydrofuran / -15 - 10 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

3.1: 1,4-dioxane / Inert atmosphere; Sealed tube

With N-Bromosuccinimide; TurboGrignard; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm400904m