ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

Base Information

Chemical Name:ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate
CAS No.:1001026-28-3
Molecular Formula:C₂₅H₂₈N₄O₆S
Molecular Weight:512.587
Hs Code.:

Synonyms:ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

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Chemical Property of ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

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Technology Process of ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

There total 1 articles about ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1001026-27-2
N-allyl-N-(benzylsulfonyl)-1-(2-cyanoethanimidoyl)-piperidine-4-carboxamide

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 1001026-28-3
ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: In ethanol; at 20 ℃; for 18h;

Reference yield: 100.0%

: 1001026-28-3
ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate

: 358-23-6
trifluoromethylsulfonic anhydride

: 1001026-32-9
ethyl 6-{4-[N-allyl-N-(benzylsulfonyl)-carbamoyl]piperidin-1-yl}-5-cyano-2-{[(trifluoromethyl)sulfonyl]oxy}nicotinate

Guidance literature:: ethyl 6-{4-[N-allyl(N-benzylsulfonyl)carbamoyl]piperidin-1-yl}-5-cyano-2-oxo-1,2-dihydropyridine-3-carboxylate; trifluoromethylsulfonic anhydride; With triethylamine; In dichloromethane; at 0 ℃; for 1h;

With water; sodium hydrogencarbonate; In dichloromethane;