(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

Base Information

Chemical Name:(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal
CAS No.:186690-20-0
Molecular Formula:C₁₇H₁₄ClFO₂S
Molecular Weight:336.814
Hs Code.:

Synonyms:(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

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Chemical Property of (Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

Chemical Property:

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Technology Process of (Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

There total 3 articles about (Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 186690-19-7
1-(4-Fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-ethanone

: 186690-20-0
(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

Guidance literature:: With trichlorophosphate; In chloroform; at 60 ℃; for 12h;

Reference yield:

: 186690-18-6
(E)-2-(4-Fluoro-phenyl)-3-(2-methoxy-4-methylsulfanyl-phenyl)-acrylic acid

: 186690-20-0
(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diphenylphosphoryl azide, triethylamine, 2.) aq. H₂SO₄ / 1.) CH₂Cl₂, r.t., 24 h, 2.) CH₂Cl₂, MeOH, r.t., 12 h

2: 100 percent / phosphorus oxychloride / CHCl₃ / 12 h / 60 °C

With sulfuric acid; diphenylphosphoranyl azide; triethylamine; trichlorophosphate; In chloroform;

Reference yield:

: 405-50-5
p-Fluorophenylacetic acid

: 186690-20-0
(Z)-3-Chloro-3-(4-fluoro-phenyl)-2-(2-methoxy-4-methylsulfanyl-phenyl)-propenal

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / acetic anhydride, triethylamine / 19 h / Ambient temperature

2: 1.) diphenylphosphoryl azide, triethylamine, 2.) aq. H₂SO₄ / 1.) CH₂Cl₂, r.t., 24 h, 2.) CH₂Cl₂, MeOH, r.t., 12 h

3: 100 percent / phosphorus oxychloride / CHCl₃ / 12 h / 60 °C

With sulfuric acid; diphenylphosphoranyl azide; acetic anhydride; triethylamine; trichlorophosphate; In chloroform;