2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

Base Information

Chemical Name:2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid
CAS No.:1434254-11-1
Molecular Formula:C₁₇H₂₃NO₇
Molecular Weight:353.372
Hs Code.:

Synonyms:2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

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Chemical Property of 2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

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Technology Process of 2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

There total 5 articles about 2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1434254-03-1
3-(tert-butyloxycarbonylamino)-4-hydroxy-1-(3,4-dimethoxyphenyl)butan-1-one

: 1434254-11-1
2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; at 30 ℃; for 15h;
DOI:10.1002/ejoc.201201128

Reference yield:

: 1434253-95-8
2-Boc-amino-3-[2-(3,4-dimethoxyphenyl)-1,3-dithian-2-yl]propan-1-ol

: 1434254-11-1
2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; iodine / acetonitrile / 1 h / 0 - 30 °C

2: dipyridinium dichromate / N,N-dimethyl-formamide / 15 h / 30 °C

With dipyridinium dichromate; iodine; sodium hydrogencarbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.201201128

Reference yield:

: 1434253-82-3
C₁₁H₂₀INO₃

: 1434254-11-1
2-(tert-butyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -20 °C

1.2: -20 °C

2.1: trifluoroacetic acid / methanol / 0 °C

3.1: sodium hydrogencarbonate; iodine / acetonitrile / 1 h / 0 - 30 °C

4.1: dipyridinium dichromate / N,N-dimethyl-formamide / 15 h / 30 °C

With dipyridinium dichromate; n-butyllithium; iodine; sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.201201128