rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine

Base Information

• Chemical Name: rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine
• CAS No.: 1273663-33-4
• Molecular Formula: C₁₆H₂₇NO
• Molecular Weight: 249.396

Synonyms:rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine

Chemical Property of rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine

Chemical Property:

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Technology Process of rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine

There total 1 articles about rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,4-di-tert-butyl-6-acetylphenol (37456-29-4) → rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine (1273663-33-4)

Guidance literature:

2,4-di-tert-butyl-6-acetylphenol; With ammonia; In methanol; at 20 ℃; for 96h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 120h;

DOI:10.1039/c4ra00414k

Reference yield:

rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine (1273663-33-4) → (R)-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / Resolution of racemate

2: hydrogenchloride / water

With hydrogenchloride; In water; acetonitrile;

DOI:10.1039/c4ra00414k

Reference yield:

rac-1-(2-hydroxy-3,5-di-tert-butylphenyl)ethylamine (1273663-33-4) + O,O'-dibenzoyl-L-tartaric acid (2743-38-6) → C16H27NO*C18H14O8 + C16H27NO*C18H14O8

Guidance literature:

In acetonitrile; Overall yield = 33 %; Resolution of racemate;

DOI:10.1039/c4ra00414k

upstream raw materials:

2,4-di-tert-butyl-6-acetylphenol

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