diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride

Base Information

• Chemical Name: diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride
• CAS No.: 1383543-07-4
• Molecular Formula: C₂₀H₂₈N₂O₂S₂
• Molecular Weight: 392.587

Synonyms:diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride

Chemical Property of diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride

Chemical Property:

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Technology Process of diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride

There total 2 articles about diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C15H18ClNO2 (1399363-05-3) + sodium N,N-diethyldithiocarbamate (148-18-5) → diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride (1383543-07-4)

Guidance literature:

In acetone; at 20 ℃; for 18h;

DOI:10.1039/c2ob25434d

Reference yield:

N-(cyclohex-1-enylmethyl)-4-methoxybenzenamine (907190-19-6) → diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride (1383543-07-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / toluene / 18 h / 20 °C

2: acetone / 18 h / 20 °C

With pyridine; In acetone; toluene;

DOI:10.1039/c2ob25434d

Reference yield: 60.0%

diethylthiocarbamic acid [4-methoxyphenyl(cyclohex-2-enyl)carbamic acid] thioanhydride (1383543-07-4) → (+/-)-(4RS,5SR)-2-(4-methoxyphenyl)-1-oxo-2-azaspiro[3.5]nonan-5-yl diethylcarbamodithioate

Guidance literature:

In cyclohexane; for 8h; Irradiation; Reflux; Inert atmosphere;

DOI:10.1039/c2ob25434d

upstream raw materials:

N-(cyclohex-1-enylmethyl)-4-methoxybenzenamine

C₁₅H₁₈ClNO₂

sodium N,N-diethyldithiocarbamate

Downstream raw materials:

2-(4-methoxyphenyl)-2-azaspiro[3.5]nonan-1-one

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