C₂₂H₁₄Br₂ClNO

Base Information

Chemical Name:C₂₂H₁₄Br₂ClNO
CAS No.:1370525-03-3
Molecular Formula:C₂₂H₁₄Br₂ClNO
Molecular Weight:503.62
Hs Code.:

C<sub>22</sub>H<sub>14</sub>Br<sub>2</sub>ClNO

Synonyms:C₂₂H₁₄Br₂ClNO

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Chemical Property of C₂₂H₁₄Br₂ClNO

Chemical Property:

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Technology Process of C₂₂H₁₄Br₂ClNO

There total 4 articles about C₂₂H₁₄Br₂ClNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1370525-03-3
C₂₂H₁₄Br₂ClNO

: 1370525-04-4
C₂₂H₁₄Br₂ClNO

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / ethanol / 6 h / Reflux

2: PPA / 2 h / 80 °C

3: p-toluenesulfonyl chloride / toluene / 1 h / 150 °C / microwave irradiation

4: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice

With sodium hydride; acetic acid; p-toluenesulfonyl chloride; In tetrahydrofuran; ethanol; toluene; mineral oil;

Reference yield:

: 1370525-02-2
C₂₁H₁₂Br₂ClNO

: 74-88-4
methyl iodide

: 1370525-03-3
C₂₂H₁₄Br₂ClNO

: 1370525-04-4
C₂₂H₁₄Br₂ClNO

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; Cooling with ice;

Reference yield:

: 1369594-43-3
C₁₄H₁₂Br₂N₂O

: 1370525-03-3
C₂₂H₁₄Br₂ClNO

: 1370525-04-4
C₂₂H₁₄Br₂ClNO

Guidance literature:: Multi-step reaction with 3 steps

1: PPA / 2 h / 80 °C

2: p-toluenesulfonyl chloride / toluene / 1 h / 150 °C / microwave irradiation

3: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Cooling with ice

With sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; toluene; mineral oil;