5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene

Base Information

• Chemical Name: 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene
• CAS No.: 125198-15-4
• Molecular Formula: C₁₇H₂₂S
• Molecular Weight: 258.428

Synonyms:5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene

Chemical Property of 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene

Chemical Property:

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Technology Process of 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene

There total 1 articles about 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzyl disulphide (150-60-7) + 1,2,3,4,5-pentamethylcyclopentadiene (4045-44-7) → 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene (125198-15-4)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, 0 deg C, 30 min, 2.) from 0 to room temp.;

DOI:10.1021/ja00159a038

Reference yield: 52.0%

maleic anhydride (108-31-6) + 5-(benzylthio)-1,2,3,4,5-pentamethylcyclopentadiene (125198-15-4) → (1S,2R,6S,7R,10S)-10-Benzylsulfanyl-1,7,8,9,10-pentamethyl-4-oxa-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (125198-18-7,125277-85-2) + (1S,2R,6S,7R,10R)-10-Benzylsulfanyl-1,7,8,9,10-pentamethyl-4-oxa-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (125198-18-7,125277-85-2)

Guidance literature:

In benzene; at 22 ℃; for 48h;

DOI:10.1021/ja00159a038

upstream raw materials:

dibenzyl disulphide

1,2,3,4,5-pentamethylcyclopentadiene

Downstream raw materials:

(1S,2R,6S,7R,10S)-10-Benzylsulfanyl-1,7,8,9,10-pentamethyl-4-oxa-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

(1S,2R,6S,7R,10R)-10-Benzylsulfanyl-1,7,8,9,10-pentamethyl-4-oxa-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

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