methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

Base Information

Chemical Name:methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate
CAS No.:179925-89-4
Molecular Formula:C₁₄H₁₄N₂O₃S
Molecular Weight:290.343
Hs Code.:

Synonyms:methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

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Technology Process of methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

There total 1 articles about methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 947-95-5
5-chloro-4-formyl-3-methyl-1-phenyl-1H-pyrazole

: 2365-48-2
Methyl thioglycolate

: 179925-89-4
methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

Guidance literature:: In methanol; at 50 ℃; for 1h;

Reference yield: 95.0%

: 179925-89-4
methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

: 24086-28-0
methyl 3-methyl-1-phenyl-1H-thieno[2,3-c]pyrazole-5-carboxylate

Guidance literature:: With sodium methylate; In methanol; at 60 - 70 ℃; for 0.5h;

Reference yield:

: 179925-89-4
methyl S-(4-formyl-3-methyl-1-phenyl-1H-pyrazol-5-yl)-2-mercaptoacetate

: 24086-27-9
3-methyl-1-phenyl-1H-thieno[2,3-c]pyrazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOCH₃ / methanol / 0.5 h / 60 - 70 °C

2: sodium hydroxide / methanol / 1.5 h / Heating

With sodium hydroxide; sodium methylate; In methanol; 1: Cyclization / 2: Hydrolysis;