chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

Base Information

Chemical Name:chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate
CAS No.:154271-40-6
Molecular Formula:C₂₀H₁₇Cl₂NO₄
Molecular Weight:406.265
Hs Code.:

Synonyms:chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

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Chemical Property of chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

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Technology Process of chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

There total 1 articles about chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 49715-04-0
chlorosulfuric acid chloromethyl ester

: 53-86-1
[1-(4-chlorobenzoyl)-5-methoxy-2-methylindol-3-yl]acetic acid

: 154271-40-6
chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

Guidance literature:: [1-(4-chlorobenzoyl)-5-methoxy-2-methylindol-3-yl]acetic acid; With sodium hydrogencarbonate; In dichloromethane; water; at 25 ℃; for 0.0333333h;

chlorosulfuric acid chloromethyl ester; In dichloromethane; at 25 ℃; for 3h; Further stages.;
DOI:10.1021/jm701450q

Reference yield: 56.0%

: 955130-62-8
O²-(acetoxymethyl) 1-[2-(hydroxycarbonyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate

: 154271-40-6
chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

: 955130-64-0
C₂₈H₂₉ClN₄O₁₀

Guidance literature:: O²-(acetoxymethyl) 1-[2-(hydroxycarbonyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate; With triethylamine; In N,N-dimethyl-formamide; at 25 ℃; for 0.166667h;

chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 40 - 45 ℃; for 17h; Further stages.;
DOI:10.1021/jm701450q