C₃₄H₂₈N₂O₂

Base Information

• Chemical Name: C₃₄H₂₈N₂O₂
• CAS No.: 180479-97-4
• Molecular Formula: C₃₄H₂₈N₂O₂
• Molecular Weight: 496.609
• Mol file: 180479-97-4.mol

Synonyms:C₃₄H₂₈N₂O₂

Chemical Property of C₃₄H₂₈N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₈N₂O₂

There total 1 articles about C₃₄H₂₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Z-1,4-dichlorobutene (1476-11-5) + (E)-1,1'-dibenzyl-[3,3'-biindolinylidene]-2,2'-dione (180479-96-3) → C34H28N2O2 (180479-97-4)

Guidance literature:

With samarium diiodide; lithium chloride; Yield given. Multistep reaction; 1.) THF, RT, 2.) THF, RT;

DOI:10.1021/ja961757m

Reference yield: 78.0%

C34H28N2O2 (180479-97-4) → C34H30N2O (180479-98-5)

Guidance literature:

With sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene; Heating;

DOI:10.1021/ja961757m

Reference yield:

C34H28N2O2 (180479-97-4) → C34H36N4O (180480-01-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 78 percent / sodium bis(2-methoxyethoxy)aluminum hydride / benzene / Heating

2: 96 percent / OsO₄, N-methylmorpholine N-oxide, H₂O / acetone; H₂O

3: 1.) Pb(OAc)4, 2.) NaBH₄ / 1.) EtOH, C₆H₆, 0 deg C

4: 87 percent / HN₃, Ph₃P, MeO₂CNNCO₂Me / tetrahydrofuran / 0 °C

5: Ph₃P, H₂O / tetrahydrofuran

With lead(IV) acetate; sodium tetrahydroborate; osmium(VIII) oxide; tris-(2-chloro-ethyl)-amine; water; 4-methylmorpholine N-oxide; dimethyl azodicarboxylate; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; water; acetone; benzene;

DOI:10.1021/ja961757m

upstream raw materials:

Z-1,4-dichlorobutene

(E)-1,1'-dibenzyl-[3,3'-biindolinylidene]-2,2'-dione

Downstream raw materials:

C₃₄H₃₀N₂O

(3aS,8aR,3'aR,8'aS)-8,8'-Dibenzyl-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]

(3aS,8aR,3'aR,8'aS)-8,8'-Dibenzyl-1,1'-dimethyl-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]

C₃₄H₃₄N₂O₃