tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

Base Information

Chemical Name:tetraethylene glycol tert-butyldiphenylsilyl tosyl diether
CAS No.:859385-34-5
Molecular Formula:C₃₁H₄₂O₇SSi
Molecular Weight:586.822
Hs Code.:

Synonyms:tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

Suppliers and Price of tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

There total 1 articles about tetraethylene glycol tert-butyldiphenylsilyl tosyl diether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 198210-37-6
2,2-dimethyl-3,3-diphenyl-4,7,10,13-tetraoxa-3-silapentadecan-15-ol

: 98-59-9
p-toluenesulfonyl chloride

: 859385-34-5
tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 3h;
DOI:10.1002/anie.200903507

Reference yield: 83.0%

: 859385-34-5
tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

: 1201411-04-2
6-((triisopropylsilyl)ethynyl)naphthalen-2-ol

: 1201411-05-3
tetraethylene glycol 6-[triisopropylsilylethynyl]-2-naphthyl tert-butyldiphenylsilyl diether

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 36h;
DOI:10.1002/anie.200903507

Reference yield:

: 859385-34-5
tetraethylene glycol tert-butyldiphenylsilyl tosyl diether

: 105-56-6
ethyl 2-cyanoacetate

: 1108168-65-5
C₂₉H₄₁NO₆Si

Guidance literature:: ethyl 2-cyanoacetate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

tetraethylene glycol tert-butyldiphenylsilyl tosyl diether; In N,N-dimethyl-formamide; at 50 ℃; for 15h; Further stages.;
DOI:10.1135/cccc20080032