1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

Base Information

Chemical Name:1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene
CAS No.:123187-16-6
Molecular Formula:C₂₁H₃₁ClO
Molecular Weight:334.93
Hs Code.:

Synonyms:1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

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Technology Process of 1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

There total 1 articles about 1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 35364-99-9
α-chlorobenzyl methyl ether

: 96806-52-9
1,1,2,2,3,3-hexamethyl-4,5-bis(methylene)cyclopentane

: 123187-16-6
1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

Guidance literature:: With zinc(II) chloride; In diethyl ether; dichloromethane; at -65 ℃; for 2h;
DOI:10.1021/jo00285a026

Reference yield:

: 123187-16-6
1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

: 110373-12-1
6,6,7,7,8,8-Hexamethyl-2,4-diphenyl-1,4,5,6,7,8-hexahydro-2H-cyclopenta[d][1,2]oxazepine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / 18 h / 85 °C

2: NaI, trimethylsilyl chloride / acetonitrile / 15 h / 85 °C

3: 98 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

4: 59 percent / toluene / 4 h / 80 °C

With chloro-trimethyl-silane; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo00285a026

Reference yield:

: 123187-16-6
1-(chloromethyl)-2-(2-methoxy-2-phenylethyl)-3,3,4,4,5,5-hexamethylcyclopentene

: 123187-20-2
5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-1,3,4,5,6,7-hexahydro-[2]pyrindine 2-oxide; compound with perchloric acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / 18 h / 85 °C

2: NaI, trimethylsilyl chloride / acetonitrile / 15 h / 85 °C

3: 98 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

4: 41 percent / methanol

With chloro-trimethyl-silane; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00285a026