C₂₂H₃₂N₄O₇S

Base Information

• Chemical Name: C₂₂H₃₂N₄O₇S
• CAS No.: 1357067-83-4
• Molecular Formula: C₂₂H₃₂N₄O₇S
• Molecular Weight: 496.585
• Mol file: 1357067-83-4.mol

Synonyms:C₂₂H₃₂N₄O₇S

Chemical Property of C₂₂H₃₂N₄O₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₂N₄O₇S

There total 1 articles about C₂₂H₃₂N₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-thiazolidine (504-78-9) + Boc-Lys(pNZ)-OH (22601-53-2) → C22H32N4O7S (1357067-83-4)

Guidance literature:

Boc-Lys(pNZ)-OH; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1h;

1,3-thiazolidine; In dichloromethane; at 0 - 20 ℃; for 18h;

Reference yield:

C22H32N4O7S (1357067-83-4) → C19H30N4O2S2 (1357143-88-4)

Guidance literature:

Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

2.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

3.1: water; lithium hydroxide monohydrate / methanol

4.1: triethylamine; methanesulfonyl chloride / dmap / dichloromethane / 20 °C

4.3: 17 h / 60 °C / Inert atmosphere

5.1: water; lithium hydroxide monohydrate / methanol

6.1: hydrogenchloride / ethanol; water

With hydrogenchloride; lithium hydroxide monohydrate; water; hydrogen; benzotriazol-1-ol; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; dmap; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; water;

Reference yield:

C22H32N4O7S (1357067-83-4) → C26H35N5O4S (1357143-90-8)

Guidance literature:

Multi-step reaction with 6 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 18 h

4: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

5: water; lithium hydroxide monohydrate / methanol

6: hydrogenchloride / ethanol; water

With hydrogenchloride; lithium hydroxide monohydrate; water; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; water;

upstream raw materials:

1,3-thiazolidine

Boc-Lys(pNZ)-OH

Downstream raw materials:

C₃₁H₄₈N₄O₈S

C₂₉H₄₆N₄O₇S

C₁₉H₃₀N₄O₃S

C₃₁H₄₈N₄O₇S₂